Crystal Structure of 4-Bromo-3,4-Dichloro-1-(1-Morpholinyl)-1-(Decylsulfanyl)-2-Nitro-Buta-1,3-Diene

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dc.contributor.authorIbis, Cemil
dc.contributor.authorDeniz, Nahide Gulsah
dc.contributor.authorTuyun, Amac Fatih
dc.date.accessioned2024-03-13T10:30:46Z
dc.date.available2024-03-13T10:30:46Z
dc.date.issued2010
dc.departmentİstanbul Beykent Üniversitesien_US
dc.description.abstractThe compound 4-bromo-3,4-dichloro-1-(1-morpholinyl)-1-(decylsulfanyl)-2-nitro-buta-3-diene was synthesized from the reaction of 4-bromo-1,3,4-trichloro-1(decylsulfanyl)-2-nitro-buta-1,3-diene with morpholine and characterized by elemental analysis, IR spectrum, UV spectra, H-1 NMR, C-13 NMR and X-ray single crystal determination. In the title compound, C18H29BrCl2N2O3S, crystallizes in the monoclinic space group P2(1)/c, a = 15.8326(4) angstrom, b = 8.9915(10) angstrom, c = 16.7528(5) angstrom, beta = 100.808(10)degrees, V = 2,342.6(3) angstrom(3), Z = 4, R-1 = 0.0590 and wR(2) = 0.0940. The morpholine ring adopts a chair conformation. The morpholine ring and the butadiene group are inclined at an angle of 113.4 (1)degrees. The butadiene unit is not planar as can be expected if the two double bonds are fully conjugated.en_US
dc.description.sponsorshipResearch Fund of Istanbul Universityen_US
dc.description.sponsorshipThe author greatly acknowledges Research Fund of Istanbul University for financial support.en_US
dc.identifier.doi10.1007/s10870-009-9660-7
dc.identifier.endpage356en_US
dc.identifier.issn1074-1542
dc.identifier.issue4en_US
dc.identifier.scopus2-s2.0-77950866090en_US
dc.identifier.scopusqualityN/Aen_US
dc.identifier.startpage353en_US
dc.identifier.urihttps://doi.org/10.1007/s10870-009-9660-7
dc.identifier.urihttps://hdl.handle.net/20.500.12662/3532
dc.identifier.volume40en_US
dc.identifier.wosWOS:000275538900012en_US
dc.identifier.wosqualityQ4en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherSpringer/Plenum Publishersen_US
dc.relation.ispartofJournal Of Chemical Crystallographyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectButadiene uniten_US
dc.subjectCrystal structureen_US
dc.subjectMorpholine ringen_US
dc.subjectChair conformationen_US
dc.titleCrystal Structure of 4-Bromo-3,4-Dichloro-1-(1-Morpholinyl)-1-(Decylsulfanyl)-2-Nitro-Buta-1,3-Dieneen_US
dc.typeArticleen_US

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